SPME-GC-FID Method Development for Analyzing Cyclohexanone Hydrogenation Products
نویسندگان
چکیده
Este trabalho apresenta o desenvolvimento de um método simples, rápido e preciso para análise dos produtos da hidrogenação eletrocatalítica da ciclohexanona com a técnica de microextração em fase sólida, usando cromatografia a gás com detector de ionização por chama. A otimização preliminar do método foi realizada através de ferramentas quimiométricas. Os resultados de LOD e LOQ foram 0,50% de conversão ou 0,78 mg L e 1,20% de conversão ou 1,86 mg L, respectivamente. A curva analítica demonstra boa linearidade (R = 0,9936).
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